TRATAMIENTO DE ABERRACIÓN ESFERICA MEDIANTE SERIE FOCAL
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Revista Boliviana de Física
Abstract
Se presenta un método iterativo para la corrección de las aberraciones de un microscopio electrónico de transmisión de alta resolución (con resolución puntual de 1.77 Å). El método se basa en la técnica de correlación de fase compensada para el alineamiento de las imágenes experimentales. La técnica empleada permitió calcular la función de onda de los electrones en el plano de salida de la muestra antes de pasar por el sistema de proyección y ser afectada por la aberración esférica de la lente objetivo. Se comprobó que la resolución fue mejorada hasta por lo menos 1.4 Å. La resolución de los "dumbbells" de silicio confirma este resultado. Se puede realizar pruebas adicionales con otros materiales para determinar la resolución alcanzada.
We present an iterative method for the correction of aberrations in an high resolution transmission electron microscope (with point resolution of 1.7 Å). The method is based on the technique of compensated phase correlation for the alignment of the experimental images. This technique helped us for calculating the wave function of electrons in the outgoing plane of the sample before passing through the projection system and be affected by the spherical aberration of the objective lens. We found that the resolution has been increased at least by 1.4 Å. The resolution of silicon dumbbells confirm this result. Additional tests with other materials can be made to determine the achieved resolution.
We present an iterative method for the correction of aberrations in an high resolution transmission electron microscope (with point resolution of 1.7 Å). The method is based on the technique of compensated phase correlation for the alignment of the experimental images. This technique helped us for calculating the wave function of electrons in the outgoing plane of the sample before passing through the projection system and be affected by the spherical aberration of the objective lens. We found that the resolution has been increased at least by 1.4 Å. The resolution of silicon dumbbells confirm this result. Additional tests with other materials can be made to determine the achieved resolution.
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Vol. 19, No. 19